Вид документа : Статья из журнала Шифр издания : 54/A 89 Автор(ы) : Timshina A.V., Rubtsova S.A., Kodess M. I., Matochkina E. G., Slepukhin P. A., Kuchin A. V. Заглавие : Asymmetrical oxidation of menthone dithiolane [Electronic resource] Место публикации : Russian Journal of Organic Chemistry (Translation of Zhurnal Organicheskoi Khimii). - 2008. - Vol. 44, № 7. - С. 1043-1048 Систем. требования: http://www.springerlink.com/content/fv42r11162161535/fulltext.pdf Примечания : 1.11.2011 г. ББК : 54 Предметные рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: Asymmetrical oxidation was performed of menthone dithiolane obtained in 95–98% yield by condensation of menthone with 1,2-ethanedithiol in the presence of boron trifluoride etherate. 6-Isopropyl-9-methyl-1,4-dithiaspiro[4,5]decane-1,4-dioxide (yield 5–55%) and 6-isopropyl-9-methyl-1,4-dithiaspiro[4,5]-decane-1,1,4-trioxide (yield 65–70%) were synthesized. Chemical structures of compounds obtained were proved by XRD analysis, NMR and IR spectroscopy Держатели документа: Центральная научная библиотека УрО РАН Доп.точки доступа: Timshina, A.V.; Rubtsova, S.A.; Kodess, M. I.; Кодесс Михаил Исаакович; Matochkina, E. G.; Slepukhin, P. A.; Kuchin, A. V.