Вид документа : Статья из журнала Шифр издания : 54/T 86 Автор(ы) : Chizhov D. L., Pervova M. G., Samorukova M. A., Khmara E. F., Filyakova V. I., Saloutin V. I., Charushin V. N. Заглавие : Trialkyl borate assisted amination of fluorinated 1,3-diketones for synthesis of N,N?-1,2-phenylen-bis(beta-aminoenones) and their Ni(II), Cu(II) and Pd(II) complexes Место публикации : Journal of Fluorine Chemistry. - 2011. - Vol. 132, № 6. - С. 394-401 Примечания : Bibliogr. : p. 401 (19 ref.) ББК : 54 Предметные рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: An effecient synthetic method for fluorinated tridentate ?-aminoenones and tetradentate bis(?-aminoenones) via amination of fluorinated 1,3-diketones with o-phenylenediamine in the presence of trialkyl borates was developed. Ni(II), Cu(II) and Pd(II) complexes with tetradentate bis(?-aminoenones) were obtained. Their gaschromatographic behaviour and main fragmentation paths in the electron ionization mass spectra were described Держатели документа: Центральная научная библиотека УрО РАН Доп.точки доступа: Chizhov, D. L.; Чижов Дмитрий Леонидович; Pervova, M. G.; Samorukova, M. A.; Khmara, E. F.; Filyakova, V. I.; Филякова Вера Ивановна; Saloutin, V. I.; Charushin, V. N.