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    (Het)aroylpyruvic acids and their derivatives as promising building blocks for organic synthesis [Electronic resource] / S. G. Perevalov, Ya. V. Burgart, V. I. Saloutin, O. N. Chupakhin // Russian Chemical Reviews. - 2001. - Vol. 70, № 11. - P921-938. - Bibliogr. : p. 938 (191 ref.)

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Methods of synthesis of (het)aroylpyruvic acids and their acyclic derivatives (esters, amides and hydrazides), and their reactions with various C-, N-, O-, S-nucleophiles are described. Problems of tautomerism and biological activity of (het)aroylpyruvates and products of their transformation are briefly considered

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    1-(Benzimidazol-2-yl)-1,2-dioxoalkane arylhydrazones and 2-phenylbenzimidazole as the main products of the reactions of 1,2,3-triketone 2-arylhydrazones with o-phenylenediamine [Electronic resource] / O. G. Khudina, N. V. Murashova, Ya. V. Burgart, V. I. Saloutin // Mendeleev Communications. - 2002. - Vol. 13, № 5. - P228-229

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: The reactions of o-phenylenediamine with 1,2,3-triketone 2-arylhydrazones containing alkyl substituents result in the predominant formation of 1-(benzimidazol-2-yl)-1,2-dioxoalkane arylhydrazones, whereas phenyl-substituted analogues afford 2-phenylbenzimidazole

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    2,3-Epoxyperfluoro-2-methylpentane in reactions with urea and thiourea [Electronic resource] / T. I. Filyakova, V. I. Saloutin, A. Ya. Zapevalov, P. A. Slepukhin, M. I. Kodess, V. I. Saloutin // Russian Journal of Organic Chemistry (Translation of Zhurnal Organicheskoi Khimii). - 2011. - Vol. 47, № 5. - P650-658 : рис., табл. - Bibliogr. : p. 658 (24 ref.)

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: 2,3-Epoxyperfluoro-2-methylpentane reacts with thiourea in protic (methanol, 2-propanol) and aprotic (dioxane) solvents, and also with urea in acetonitrile affording unexpected products: 1-(2,2,3,3,3-pentafluoropropionyl)-2-(2,2,2-trifluoro-1-trifluoro-methylethyl)isothiourea, and 1-(2,2,3,3,3-pentafluoropropionyl)-3-(2,2,2-trifluoro-1-trifluoro-methylethyl)urea respectively that result from the rearrangement of the intermediately formed ketone in the process of the intramolecular “haloform” cleavage. At the same time in dioxane the 2,3-epoxyperfluoro-2-methylpentane reacts with urea with the formation of a heterocyclic compound, 2-amino-4-pentafluoroethyl-5,5-bis(trifluoromethyl)-4,5-dihydrooxazol-4-ol. From 1-(2,2,3,3,3-pentafluoropropionyl)-2-(2,2,2-trifluoro-1-trifluoromethylethyl)isothiourea and Cu(OAc)2 a stable fluorine-containing chelate complex was obtained

\\\\Expert2\\nbo\\Russian Journal of Organic Chemistry\\2011, 47 (5), 650-658.pdf
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    2-(Het)arylhydrazono-1,3-dicarbonyl compounds in organic synthesis [Electronic resource] / E. V. Shchegol'kov, Ya. V. Burgart, O. G. Khudina, V. I. Saloutin, O. N. Chupakhin // Russian Chemical Reviews. - 2010. - Vol. 79, № 1. - P31-62 : рис.

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: The data on the synthesis, structure and chemical transformations of 2-(het)arylhydrazono-1,3-dicarbonyl compounds is surveyed. The synthetic potential and possible applications of the title compounds are analyzed

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    3-(2-Arylhydrazono)-1,1,1-trifluro-3-(phenylsulfonyl)propan-2-ones as selective carboxylesterase inhibitors / E. V. Shchegolkov, Y. V. Burgart, N. A. Elkina [et al.] // Russian chemical bulletin. - 2022. - Vol. 71, № 1. - P158-164
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: We improved the synthetic procedure for 3-(2-arylhydrazono)-1,1,1-trifluro-3-(phenylsulfonyl)propan-2-ones and established their structure. The study of their esterase profile showed the absence of cholinesterase inhibition and the selectivity against carboxylesterase with micromolar activity exceeding the anticarboxylesterase activity of the diketone analog. Carboxylesterase inhibition data are consistent with molecular docking results. 3-(2-Arylhydrazono)-1,1,1-trifluro-3-(phenylsulfonyl)propan-2-ones exhibit a high radical-scavenging effect in the ABTS test exceeding that of Trolox.

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    3-Methylidene-2,4-dioxo-4-pentafluorophenylbutanoates in the Synthesis of Heterocycles [Electronic resource] / A. S. Fokin, Ya. V. Burgart, V. I. Saloutin, O. N. Chupakhin // Russian Journal of Organic Chemistry (Translation of Zhurnal Organicheskoi Khimii). - 2005. - Vol. 41, № 9. - P1354-1358

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: 3-Ethoxy- and 3-arylaminomethylidene-2,4-dioxo-4-pentafluorophenylbutanoates undergo cyclization by the action of hydrazine hydrate and phenylhydrazine to give ethyl 4-pentafluorobenzoylpyrazole-5-carboxylates. The reaction of 3-ethoxymethylidene-2,4-dioxo-4-pentafluorophenylbutanoate with o-phenylene-diamine leads to formation of 3-[2-(2-aminophenylamino)-1-pentafluorobenzoylethenyl]-1,2-dihydroquinoxa-lin-2-one. 3-Arylaminomethylidene-2,4-dioxo-4-pentafluorophenylbutanoates react with o-phenylenediamine to afford 3-(1-aryl-5,6,7,8-tetrafluoro-4-oxo-1,4-dihydroquinolin-3-yl)-1,2-dihydroquinoxalin-2-ones and/or 3-(2-arylamino-1-pentafluorobenzoylethenyl)-1,2-dihydroquinoxalin-2-ones

\\\\Expert2\\nbo\\Russian Journal of Organic Chemistry\\2005, 41 (9), 1374-1376.pdf
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   П 99


    5,6,7,8-Tetrafluoro-4-hydroxycoumarin derivatives in reactions with o-phenylenediamine [Electronic resource] / Ya. V. Burgart, K. V. Shcherbakov, V. I. Saloutin, O. N. Chupakhin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2004. - Vol. 53, № 6. - P1237-1239. - Библиогр. : с. 1239 (5 назв.)

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
TETRAFLUORO -- HYDROXYCOUMARINES
Аннотация: The reactions of 5,6,7,8-tetrafluoro-4-hydroxycoumarin derivatives with o-phenylenediamine occur with pyrone heterocycle cleavage and formation of substituted benzodiazepin-2-ones. 5,6,7,8-Tetrafluoro-4-hydroxycoumarin affords 4-(3,4,5,6-tetrafluoro-2-hydroxyphenyl)-2,3-dihydro-1H-1,5-benzodiazepin-2-one, 3-acetimidoyl-5,6,7,8-tetrafluoro-4-hydroxycoumarin produces 3-(3,4,5,6-tetrafluoro-2-hydroxybenzoyl)-4-methyl-1,2-dihydro-1H-1,5-benzodiazepin-2-one, and 3-acetyl-5,6,7,8-tetrafluoro-4-hydroxycoumarin yields both these heterocycles.

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2004, 53 (6), 1237-1239.pdf
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    6-Polyfluoroalkylated 2-thiouracils in the synthesis of pyrimido[2,1-b][1,3,5]thiadiazines by the double Mannich reaction [Electronic resource] / O. G. Khudina, A. E. Ivanova, Ya. V. Burgart, V. I. Saloutin, M. A. Kravchenko // Journal of Fluorine Chemistry. - 2013. - Vol.147. - P31-35

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
ALIPHATIC AND AROMATIC AMINES -- ETHYLENEDIAMINE -- FORMALDEHYDE
Аннотация: 6-Polyfluoroalkyl-2-thiouracils react with formaldehyde and primary amines in EtOH (MeCN) at 2-mercapto and 3-amino groups to yield pyrimido[2,1-b][1,3,5] thiadiazines via the multicomponent double Mannich reaction. The structure of 3-benzyl-8-nonafluorobutyl-3,4-dihydro-2H,6H-pyrimido[2,1-b][1,3,5] thiadiazin-6-one was studied by the X-ray diffraction analysis. The use of ethylenediamine in these reactions yields 3,3′-ethane-1,2-diyl- bis(pyrimido[2,1-b]thiadiazinone) as a result of the bis-double Mannich cyclocondensation. 8-Polyfluoroalkyl-pyrimido[2,1-b]thiadiazines exhibit weak tuberculostatic activity

\\\\Expert2\\NBO\\Journal of Fluorine Chemistry\\2013, v. 147, p.31.pdf
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   A 10


    A concise approach to CF3-containing furan-3-ones, (bis)pyrazoles from novel fluorinated building blocks based on 2,3-butanedione [Electronic resource] / D. N. Bazhin, G. -V. Roeschenthaler, D. L. Chizhov, Yu. S. Kudyakova, Ya. V. Burgart, P. A. Slepukhin, V. I. Saloutin, V. N. Charushin // Tetrahedron Letters. - 2014. - Vol. 55. - С. 5714-5717. - Bibliogr. : p. 5717 (16 ref.)

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
ClISEN CONDENSATION -- AKOXYENONES; -- TRIFLUOROACETYLATION
Аннотация: 1,1,1-Trifluoro-4,5,5-trimethoxyhex-3-en-2-one and lithium (2Z)-1,1,1-trifluoro-5,5-dialkoxy-4-oxohex-2-en-2-olate were synthesized for the first time via direct trifluoroacetylation of 2,3-butanedione acetal derivatives. A simple and effective approach to acetal or acyl substituted CF3-pyrazoles, 5,5′-bis(trifluoromethyl)-3,3′-bipyrazole, and, to 5-trifluoromethylfuran-3-ones is presented.

\\\\expert2\\nbo\\Tetrahedron Letters\\2014, v. 55, p. 5714.pdf
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10.

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   A 10


    A convenient approach to 4,7-dihydrotetrazolo [5,1-c ][1,2,4]triazine synthesis [Electronic resource] / E. V. Shchegol'kov, A. E. Ivanova, Ya. V. Burgart, V. I. Saloutin // Journal of Heterocyclic Chemistry. - 2013. - Vol.50. - PE80-E86

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
TRIAZINE SYNTHESIS -- 1,3-DICARBONYL -- ISOMERISM
Аннотация: Azo coupling of 1,3-dicarbonyl compounds with tetrazolyl-5-diazonium chloride is used to develop a convenient one-step procedure for the synthesis of 4,7-dihydrotetrazolo[5,1-c][1,2,4]triazines. In contrast to nonfluorinated analogs, 7-hydroxy-7-polyfluoroalkyl-4,7-dihydrotetrazolo[5,1-c][1,2,4]triazines undergo a ring-chain isomerism resulting from the cleavage at the C7 - N7a bond. A distinctive feature of nonfluorinated 4,7-dihydrotetrazolo[5,1-c][1,2,4] triazines is the possibility to dehydration, which is accompanied by an azide rearrangement due to the tetrazole ring cleavage with the formation of tetrazolo[1,5-b][1,2,4]triazines

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11.

Инвентарный номер: нет.

   A 10


    A Convenient Approach to CF3-Containing N-Heterocycles Based on 2-Methoxy-2-methyl-5-(trifluoromethyl)furan-3(2H)-one [Electronic resource] / D. N. Bazhin, Yu. S. Kudyakova, G. -V. Roeschenthaler, Ya. V. Burgart, P. A. Slepukhin, M. L. Isenov, V. I. Saloutin, V. N. Charushin // European Journal of Organic Chemistry. - 2015. - № 23. - С. 5236-5245. - Bibliogr. : p. 5245 (23 ref.)

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
NITROGEN HETEROCYCLES -- FLUORINE -- OXYGEN HETEROCYCLES
Аннотация: New synthetic routes to trifluoromethylated N-heterocycles based on condensations of 2-methoxy-2-methyl-5-(trifluoromethyl)furan-3(2H)-one with bifunctional N-nucleophiles are described. For the first time, trifluoromethyl-containing pyrazoles, pyrazolines and isoxazolines bearing hydrazone or oxime groups could be obtained by a one-pot strategy based on reactions of 5-(trifluoromethyl)furan-3(2H)-one with two equivalents of the corresponding hydrazines or hydroxylamine in the presence of an acid. The interaction of furan-3(2H)-one with ureas proceeded under mild conditions to furnish 1H-furo[2,3-d]imidazol-2(3H)-one derivatives in good yield. Further, a trifluoromethyl-containing quinoxaline derivative was obtained by condensation of furan-3(2H)-one with ortho-phenylenediamine.

\\\\expert2\\nbo\\European Journal of Organic Chemistry\\2015, №23. p.5236-5245.pdf
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12.

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   A 10


    A new application of derivatives of polychlorobiphenyls and polyethylene glycols / T. I. Gorbunova, M. G. Pervova, E. B. Trushina, S. V. Pavlysko, A. Ya. Zapevalov, V. I. Saloutin // Russian Journal of Applied Chemistry. - 2012. - Vol.85, №10. - С. 1622-1626

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
POLYCHLOROBIPHENYLS -- POLYETHYLENE GLYCOLS -- SYNTHESIS
Аннотация: The reaction of congeners of Sovol technical mixture of polychlorobiphenyls with polyethylene glycols was studied. Mixtures of hydroxy and mono(polyethylene glycol)oxy derivatives were obtained. The mixtures synthesized, which are of low hazard, were used as additives to industrial oil to improve its tribological char

\\\\Expert2\\nbo\\Russian Journal of Applied Chemistry\\2012, v. 85, N 10, p.1662.pdf
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13.

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   A 10


    A new approach to the synthesis of fluorinated chromones [Electronic resource] / V. I. Saloutin, I. T. Bazyl, Z. E. Skryabina, V. M. Krokhalev, O. N. Chupakhin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 1992. - Vol. 41, N 9. - P1714-1715

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: The condensation of two molecules of ethyl pentafluorobenzoylacetate gives 1-oxo-3-penta fluorophenyl-1H-pyrano[4,3-b]6,7,8,9-tetrafluorochrome

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\1992, 41 (9), 1714.pdf
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14.

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   A 10


    A Novel Route to the Synthesis of Fluoroalkylated Hexahydroimidazo[1,2-a]pyridines [Text] / Yu. S. Kudyakova, M. V. Goryaeva, Ya. V. Burgart, V. I. Saloutin // IV International Conference "Multi-Component Reactions and Related Chemistry", Ekaterinburg, 24-28 May 2009. - Екатеринбург, 2009. - PS 22

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ

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15.

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   A 10


    A route to ethyl alfa-pentafluorobenzoyl-beta-oxobutanoate via its copper(II) chelate [Text] / Ya. V. Burgart, S. P. Kisil', V. I. Saloutin, O. N. Chupakhin // Mendeleev Communications. - 2001. - Vol. 11, № 2. - P76

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Ethyl 2-pentafluorobenzoyl-3-oxobutanoate has been prepared by the acylation of ethyl acetoacetate with pentafluorobenzoyl chloride via a copper(II) chelate

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16.

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   A 10


    A route to fluorocontaining 1,3-thiazolines via internal polyfluorooxiranes [Electronic resource] / L. V. Saloutina, A. Ya. Zapevalov, M. I. Kodess, V. I. Saloutin, O. N. Chupakhin // Mendeleev Communications. - 1999. - N 6. - P231-232 . - ISSN 0959-9436

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: The reaction of internal fluoroolefin oxides with thiourea results in 2-amino-5-fluoro-4-hydroxy-4,5-di(polyfluoroalkyl)-1,3-thiazolines, providing a route to an unknown type of fluorine-containing thiazolines with two fluoroalkyl substituents

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17.

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   A 10


    A route to fluorocontaining N,S-heterocycles via octafluoro-2,3-epoxybutane [Text] / L. V. Saloutina, A. Ya. Zapevalov, V. I. Saloutin, P. A. Slepukhin, M. I. Kodess, V. E. Kirichenko, M. G. Pervova, O. N. Chupakhin // Journal of Fluorine Chemistry. - 2007. - Vol. 128, № 7. - P769-778

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: The reaction of octafluoro-2,3-epoxybutane 1 with 2-aminothiophenol gave three kinds of novel fluorocontaining N,S-heterocyclic compounds depending on the solvent nature: 2,3-bis(trifluoromethyl)-3,4-dihydro-2H-1,4-benzothiazin-2-ol 2, 2-trifluoromethyl-2-[1-(2-aminophenylthio)-2,2,2-trifluoroethyl]-1,3-benzothiazolidine 6 and 5a,11a-bis(trifluoromethyl)-5a,6,11a,12-tetrahydro-5,11-dithia-6,12-diazanaphthacene 5. Use of the toluene, dioxane, tetrahydrofuran, acetonitrile and dimethoxyethane gave the unexpected dihydrobenzothiazine 2 (RS,SR RR,SS) in good to moderate yields. In dimethylsulfoxide and N,N-dimethylacetamide, unusual cyclization occurred resulting in benzothiazolidine 6 (RS,SR/RR,SS 1:1) in moderate yields. Formation of minor 1,1,1,3,4,4,4-heptafluoro-3-(2-aminophenylthio)-2,2-dihydroxybutane 4 which was converted into bis(benzothiazine) 5 was observed in all solvents tested with the exception of toluene and dioxane. The molecular structure of the RS,SR-diastereomer of dihydrobenzothiazine 2, bis(benzothiazine) 5 and the RS,SR-diastereomer of benzothiazolidine 6 has been established by X-ray crystallography.

\\\\Expert2\\nbo\\Journal of Fluorine Chemistry\\2007, v.128. p.769.pdf
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18.

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   A 10


    A study of the physico-chemical features of the [(perfluoroalkyl)methyl]oxirane amino derivatives based on the hexafluoropropylene oxide trimer / D. N. Bazhin, T. I. Gorbunova, A. Ya. Zapevalov, I. V. Beketov, V. I. Saloutin // Russian Journal of General Chemistry. - 2011. - Vol.81, №9. - С. 1829-1833

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
PHYSICO-CHEMICAL FEATURES -- HEXAFLUOROPROPYLENE -- OXIDE TRIMER
Аннотация: The 1,2-epoxy-4,6,6,7,9,9,10,10,11,11,11-undecafluoro-4,7-bis(trifluoromethyl)-5,8-dioxaundecane was synthesized for the first time on the basis of the hexafluoropropylene oxide trimer. We showed that it reacted with diethylamine, morpholine, or N-methylpiperazine to afford the product of regioselective cleavage of the oxirane ring. The processing of nano-sized copper powder with a solution of the obtained hydroxyamine solution in acetone allowed the formation of the hydrophobic metal coating

\\\\Expert2\\nbo\\Russian Journal of General Chemistry\\2012, V. 81, N 9, p. 1829–1833.pdf
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19.

Инвентарный номер: нет.

   A 20


    Addition of polyfluoroalkyl iodides to allyl glycidyl ether [Electronic resource] / D. N. Bazhin, T. I. Gorbunova, A. Ya. Zapevalov, V. I. Saloutin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2007. - Vol. 56, № 8. - P1534-1536. - Библиогр. : с. 1536 (24 назв.)

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Addition of polyfluoroalkyl iodides to the double bond of allyl glycidyl ether occurred under mild conditions (20-25 °C, MeCN/H2O, Na2S2O4, NaHCO3) with retention of the oxirane ring.

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2007, 56 (8), 1534-1536.pdf
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20.

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   A 25


    Aggregative stability of the CdS nanoparticles-H2O colloidal dispersion system in the presence of surfactants / N. S. Kozhevnikova, T. I. Gorbunova, A. S. Vorokh, D. N. Bazhin, A. Ya. Zapevalov, V. I. Saloutin, A. A. Rempel, O. N. Chupakhin // Doklady Chemistry. - 2012. - Vol.443, №1. - С. 86-90

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
CdS -- COLLOIDAL DISPERSION SYSTEM -- AGGREGATIVE STABILITY

\\\\Expert2\\nbo\\Doklady Chemistry\\2012, v. 443, N 1, p. 86-90.pdf
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21.

Инвентарный номер: нет.

   A 37


    Alkyl 3-fluoroalkyl-3-oxopropionates in reactions with azolyldiazonium salts [Electronic resource] / E. V. Shchegol'kov, E. V. Sadchikova, Ya. V. Burgart, V. I. Saloutin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2008. - Vol. 57, № 3. - P612-618

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Alkyl 3-fluoroalkyl-3-oxopropionates react with antipyrinyldiazonium chloride to form 2-antipyrinylhydrazono-3-fluoroalkyl-3-oxopropionates. The use in these reactions of hetaryldiazonium salts, containing NH group in the ? position, leads to alkyl 7-fluoroalkyl-7-hydroxy-4,7- dihydroazolo[5,1-c]triazine-6-carboxylates. 3-Amino-1H-1,2,4-triazole, 3-amino-4-ethoxycar- bonyl-1H-pyrazole, and 5-amino-4-ethoxycarbonyl-1H-imidazole were used as the heterocyclic component

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2008, 57 (3), 612.pdf
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22.

Инвентарный номер: нет.



    Alternative approaches to the synthesis of polyfluoroalkyl-containing 1-methyl-4-nitrosopyrazoles / N. A. Agafonova, Y. V. Burgart, N. A. Gerasimova [et al.] // Russian chemical bulletin. - 2021. - Vol. 70, № 6. - P1135–1140
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
4,4,4-TRIFL UORO-3,3-DIHYDROXY-2-(HYDROXYIMINO)BUTAN-1-ONES -- POLYFL UOROALKYL2-HYDROXYIMINO-1,3-DIKETONES -- 1-METHYL-4-NITROSOPYRAZOLES -- MYCOSTATIC ACTIVITY
Аннотация: We studied different approaches to the synthesis of polyfluoroalkyl-containing 1-methyl-4-nitrosopyrazoles, which are based on the cyclization of 4,4,4-trifluoro-3,3-dihydroxy-2-hydroxyimino-1-R-butan-1-ones or 2-hydroxyimino-1,3-diketones with methylhydrazine and on a one-pot sequential treatment of 1,3-diketones with sodium nitrite and methylhydrazine. It was found that the regioselectivity of the formation of 1-methyl-4-nitrosopyrazoles is affected by the steric factors of 1,3-dicarbonyl reagents. The study of the mycostatic effect of 4-nitrosopyrazoles showed that the introduction of a bulky polyfluoroalkyl or tert-butyl substituent leads to a decrease in their activity.

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23.

Инвентарный номер: нет.

   A 53


    An interdisciplinary approach to the problem of neutralization of man-made polychlorinated biphenyls [Electronic resource] / T. I. Gorbunova, M. G. Pervova, A. A. Panyukova, D. O. Egorova, V. I. Saloutin, V. A. Demakov, O. N. Chupakhin // Doklady Chemistry. - 2014. - Vol.454, №2. - С. 19-24. - Bibliogr. : p. 24 (15 ref.)

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
POLYCHLORINATED BIPHENYLS -- BACTERIAL DEGRADATION

\\\\expert2\\nbo\\Doklady Chemistry\\2014, v. 454, N 2, p.19-24.pdf
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24.

Инвентарный номер: нет.

   A 62


    Antifriction properties of fluorine-containing poly(ethylene glycol) esters / T. I. Gorbunova, D. N. Bazhin, A. Ya. Zapevalov, L. G. Korshunov, I. V. Beketov, V. I. Saloutin // Russian Journal of Applied Chemistry. - 2012. - Vol.85, №2. - С. 267-271

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
ANTIFRICTION PROPERTIES -- FLUORINE-CONTAINING POLY(ETHYLENE GLYCOL) ESTERS -- EQUILIBRIUM MIXTURES
Аннотация: Equilibrium mixtures of fluorine-containing mono- and diesters based on poly(ethylene glycol) (M = 1000) were synthesized. The effect of these compounds on antifriction properties of industrial oil was studied

\\\\Expert2\\nbo\\Russian Journal of Applied Chemistry\\2012, v. 85, N 2, p.267.pdf
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25.

Инвентарный номер: нет.

   A 62


    Antifriction properties of new fluorine-containing derivatives of natural graphite / T. I. Gorbunova, A. Ya. Zapevalov, D. N. Bazhin, L. G. Korshunov, V. S. Gaviko, V. I. Saloutin // Russian Journal of Applied Chemistry. - 2012. - Vol.85, №1. - С. 102-107

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
ANTIFRICTION PROPERTIES -- FLUORINE-CONTAINING DERIVATIVES -- GRAPHITE
Аннотация: Interaction of natural graphite with potassium salts of perfl uoro(ω-chloroperfl uoro)carboxylic acids in the presence of potassium persulfate was studied. The derivatives obtained were used as independent lubricants for a chromium-containing-steel friction pair

\\\\Expert2\\nbo\\Russian Journal of Applied Chemistry\\2012, v. 85, N 1, p.102.pdf
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26.

Инвентарный номер: нет.

   A 89


    Asymmetric azomethine ligands based on 2-[(2-aminophenyl)aminomethylidene]-3-oxo-3-polyfluoroalkylpropionates and aldehydes [Electronic resource] / Yu. S. Kudyakova, M. V. Goryaeva, Ya. V. Burgart, V. I. Saloutin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2010. - Vol. 59, № 9. - P1753-1760 : рис., табл. - Bibliogr. : p. 1759-1760 (12 ref.)

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
AZOMETHINES -- ALDEHYDES -- LIGANDS -- NICKEL(II) COMPLEXES -- COPPER(II) COMPLEXES -- ORGANOFLUORINE COMPOUNDS -- X-RAY DIFFRACTION STUDY
Аннотация: The condensation of ethyl 2-[(2-aminophenyl)aminomethylidene]-3-oxo-3-polyfluoroalkyl-propionates with aldehydes (salicylaldehyde, furfural, and benzaldehyde) affords the corresponding azomethine derivatives exhibiting the complexing ability toward copper and nickel ions.

\\\\Expert2\\nbo\\Russian Chemical Bulletin\\2010, 59 (9), 1753-1760.pdf
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27.

Инвентарный номер: нет.

   B 57


    Biginelli condensations of fluorinated 3-oxo esters and 1,3-diketones [Text] / V. I. Saloutin, Ya. V. Burgart, O. G. Kuzueva, C. O. Kappe, O. N. Chupakhin // Journal of Fluorine Chemistry. - 2000. - Vol. 103, № 3. - P17-23

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Аннотация: Condensation of fluorinated 3-oxo esters or 1,3-diketones with benzaldehyde and (thio)urea results in the diastereoselective formation of 4-fluoroalkyl-4-hydroxy-2-oxo(thioxo)-6-phenyl-hexahydropyrimidine-5-carboxylates from which by dehydration under acidic conditions the corresponding 6-fluoroalkyl-2-oxo(thioxo)-4-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylates were obtained. Under the same conditions, hexafluoroacetylacetone furnishes 4,6-dihydroxy-4,6-di(trifluoromethyl)-hexahydropyrimidin-2-one. Some further reactions of these pyrimidine derivatives leading to fused heterocycles are described.????

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28.

Инвентарный номер: нет.

   B 62


    Bis(1,1,1,3,5,5,5-heptafluoro-4-iminopent-2-ene-2-aminato)copper(ii) — a new metal-containing matrix in the design of heterospin systems [Electronic resource] / S. V. Fokin, V. Ovcharenko, G. V. Romanenko, E. V. Tretyakov, A. S. Bogomyakov, V. I. Saloutin, T. I. Filyakova, L. V. Saloutina, V. N. Charushin, O. N. Chupakhin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2011. - Vol.60, №5. - С. 816-823. - Bibliogr. : p. 823 (11 ref.)

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
COPPER(II) -- BISCHELATES -- NITROXIDES
Аннотация: The first heterospin compounds based on bis(1,1,1,3,5,5,5 heptafluoro 4 iminopent 2 ene 2 aminato)copper(II) (CuL2) and nitronyl nitroxide radicals, 2 R 4,4,5,5 tetramethyl 4,5 dihydro 1H imidazole 3 oxide 1 oxyls (NIT R, where R = H, Me, Ph, and 1 methyl pyrazol 4 yl), were synthesized and structurally characterized. An important peculiarity of the structure of synthesized solid phases is the formation of a supramolecular structure due to hydrogen bonds between the oxygen atoms of the nitronyl nitroxide fragments of NIT R and the hydrogen atoms of the NH groups of CuL2

\\\\expert2\\NBO\\Russian Chemical Bulletin\\2011, 60 (5), 816-823.pdf
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29.

Инвентарный номер: нет.

   B 96

    Burgart, Ya. V.
    Fluorine-containing 2-functionalized 1,3-dicarbonyl compounds for heterocyclic synthesis [Text] / Ya. V. Burgart, V. I. Saloutin, O. N. Chupakhin // Heterocycles. - 2006. - Vol. 69, № 1. - P593-620

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
FLUORINE-CONTAINING

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30.

Инвентарный номер: нет.

   B 96

    Burgart, Ya. V.
    Ring-chain isomerism of 7-Fluoroalkyl-4,7-dihydroazolo[1,5-a]pyrimidines [Text] : доклад, тезисы доклада / Ya. V. Burgart, M. V. Pryadeina, V. I. Saloutin // 15th European symposium on fluorine chemistry, Prague, Czech Republic, July 15-20, 2007 : abstr. - 2007. - P192

ББК 54
Рубрики: ХИМИЧЕСКИЕ НАУКИ
Кл.слова (ненормированные):
7-FlUOROALKYL-4,7-DIHYDROAZOLO[1,5-A]PYRIMIDINES -- RING-CHAIN ISOMERISM

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