S 67 Slepukhin, P. A. X-ray structural investigation of the products of ring closure of 2-alkenylthiopyridines upon treatment with mercury iodide [Electronic resource] / P. A. Slepukhin, D. G. Kim, V. N. Charushin // Journal of Structural Chemistry. - 2008. - Vol. 49, № 6. - P1144-1148 Рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: The products of the reaction of 2-alkenylthiopyridines with mercury iodide have been studied by single crystal X-ray diffraction. It has been demonstrated that the products are organomercury derivatives of salts of 2,3-dihydrothiazolo[3,2-a]pyridinium \\\\Expert2\\nbo\\Journal of Structural Chemistry\\2008, V. 49, N 6, p.1144.pdf |
S 67 Slepukhin, P. A. Structural study of the CoCl2 complex with 8(-2-butylthioethyl)oxyquinoline [Electronic resource] / P. A. Slepukhin, D. G. Kim, V. N. Charushin // Russian Journal of Coordination Chemistry. - 2010. - Vol. 36, № 8. - P615-617 Рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: Complex [CoCl(L)]2(Cl)2 (L = 8-(2-butylthioethyl)oxyquinoline) is studied by X-ray diffraction analysis. The empirical formula of the compound is C30H34Cl4Co2N2O2S2, the crystals are monoclinic, a = 9.9382(13) A, b = 11.9097(8) A, c = 14.5715(11) A = 102.511(9)°, Z = 2, space group P21/c. The complex is dimeric with bridging chlorine atoms, and the heterocyclic ligand L is tridentate-cyclic \\\\Expert2\\nbo\\Russian Journal of Coordination Chemistry\\2010, v. 36, N. 8, p.615.pdf |
S 98 Synthesis of 6,7-dihydro-5H-[1,3,4]thiadiazolo-[2,3-b][1,3]thiazinium system derivatives [Electronic resource] / D. G. Kim, N. M. Sudolova, P. A. Slepukhin, V. N. Charushin // Chemistry of Heterocyclic Compounds. - 2011. - Vol. 46, № 11. - P1420-1421. - Bibliogr. : p. 1421 (3 ref.) Рубрики: ХИМИЧЕСКИЕ НАУКИ \\\\Expert2\\nbo\\Chemistry of Heterocyclic Compounds\\2011, v.46, N 11, p.1420-1421.pdf |
K 45 Kim, D. G. Tandem heterocyclization in the synthesis of novel imidazo[1,5-d][1,3,4]thiadiazine / D. G. Kim, E. S. Ilinykh, P. A. Slepukhin // Chemistry of Heterocyclic Compounds. - 2011. - Vol. 46, № 11. - P1418-1419 Рубрики: ХИМИЧЕСКИЕ НАУКИ Кл.слова (ненормированные): 1,3,4-THIADIAZOLE -- 7-AMINO -- THIADIAZINIUM PENTAIODIDE \\\\Expert2\\nbo\\Chemistry of Heterocyclic Compounds\\2011, v.46, N 11, p.1418-1419.pdf |
T 19 Tandem reactions in the iodination of 2-(2-bromoallyl)thioquinoline / E. A. Vershinina, D. G. Kim, P. A. Slepukhin // Chemistry of Heterocyclic Compounds. - 2011. - Vol. 46, № 11. - P1415-1417. - Bibliogr. : p. 1417 (3 ref.) Рубрики: ХИМИЧЕСКИЕ НАУКИ Кл.слова (ненормированные): 2-QUINOLINETHIONE -- [3,2-a]QUINOLINIUM IODIDE -- 1-METHYLIDENE \\\\Expert2\\nbo\\Chemistry of Heterocyclic Compounds\\2011, v.46, N 11, p.1415-1417.pdf |
F 94 Frolova, T. V. Heterocyclization of 5-ethyl- 2-methallylthio-6-methyl-4(3H)-pyrimidinone using acids / T. V. Frolova, P. A. Slepukhin, D. G. Kim // Chemistry of Heterocyclic Compounds. - 2011. - Vol. 47, № 2. - P252-254. - Bibliogr. : p. 253-254 (6 ref.) Рубрики: ХИМИЧЕСКИЕ НАУКИ Кл.слова (ненормированные): X-RAY STRUCTURAL ANALYSIS ???? -- 4(3H)-PYRIMIDINONES -- HETERO-CYCLIZATION \\\\Expert2\\nbo\\Chemistry of Heterocyclic Compounds\\2011, v.47, N 2, p.252-254.pdf |
K 45 Kim, D. G. Investigation of the halocyclization of S- and N-allyl derivatives of 2-benzothiazolethione / D. G. Kim, N. M. Sudolova, P. A. Slepukhin // Chemistry of Heterocyclic Compounds. - 2011. - Vol. 47, № 5. - P631-635. - Bibliogr. : p. 635 (11 ref.) Рубрики: ХИМИЧЕСКИЕ НАУКИ Кл.слова (ненормированные): X-RAY CRYSTALLOGRAPHY -- HALOCYCLIZATION -- 3-HALOMETHYL \\\\Expert2\\nbo\\Chemistry of Heterocyclic Compounds\\2011, v.47, N 5, p.631-635.pdf |
A 10 A single crystal X-ray study of the products of halogen mercury cyclization of 8-allylthioquinoline / P. A. Slepukhin, V. I. Batalov, D. G. Kim, V. N. Charushin // Journal of Structural Chemistry. - 2012. - Vol.53, №1. - С. 145-150 Рубрики: ХИМИЧЕСКИЕ НАУКИ Кл.слова (ненормированные): 8-ALLYLTHIOQUINOLINE -- X-RAY DIFFRACTION -- HALOGEN Аннотация: The reaction products of 8-allylthioquinoline with mercury halides are studied by single crystal X-ray diffraction. It is shown that the products are organomercury derivatives of salts of 2,3-dihydro[1,4]-thiazino[2,3,4-ij]quinoliniuim \\\\Expert2\\nbo\\Journal of Structural Chemistry\\2012, V. 53, N 1, p.145-150.pdf |
S 98 Synthesis of novel fluorine- and iodine-containing [1,2,4]triazolo[3,4-b][1,3]thiazines based 3-(alkenylthio)-5-(trifluoromethyl)-4H-1,2,4-triazole-3-thiols [Electronic resource] / E. S. Ilinykh, D. G. Kim, M. I. Kodess, E. G. Matochkina, P. A. Slepukhin // Journal of Fluorine Chemistry. - 2013. - Vol.149. - P24-29 Рубрики: ХИМИЧЕСКИЕ НАУКИ Кл.слова (ненормированные): SYNTHESIS -- FLUORINE-CONTAINING -- IODIDES Аннотация: In this paper we report the synthesis of novel S-alkenyl derivatives of 5-(trifluoromethyl)-4H-1,2,4-triazole-3-thiol via alkenation reaction with different alkenyl halides. Reaction between the resulting S-alkenation products and iodine proceeds regiospecifically to give new fused fluorine- and iodine-containing [1,2,4]triazolo[3,4-b][1,3]thiazine heterocyclic systems. The structure of synthesized compounds was confirmed by mass spectra, IR, 1H, 13C and 19F NMR spectroscopy including 2D 1H–13C HSQC, 1H–1H COSY, 1H–13C HMBC correlations, elemental analysis and single-crystal X-ray diffraction study. -------------------------------------------------------------------------------- \\\\Expert2\\NBO\\Journal of Fluorine Chemistry\\2013, v. 149, p.24.pdf |
V 50 Vershinina, E. A. Synthesis of oxazolo[3,2-a]quinolinium triiodide from 4-methyl-1-(3-methylbut-2-enyl)quinolin-2(1H)-one [Electronic resource] / E. A. Vershinina, P. A. Slepukhin, D. G. Kim // Chemistry of Heterocyclic Compounds. - 2012. - Vol.47, №12. - P1596-1597 Рубрики: ХИМИЧЕСКИЕ НАУКИ Кл.слова (ненормированные): SYNTHESIS -- TRIIODIDE -- QUINOLINE \\\\Expert2\\NBO\\Chemistry of Heterocyclic Compounds\\2011, v.47, N 12, p.1596-1597.pdf |
C 73 Complex structure tri- and polyiodides of iodocyclization products of 2-allylthioquinoline [Electronic resource] / E. V. Bartashevich, I. D. Yushina, E. A. Vershinina, P. A. Slepukhin, D. G. Kim // Journal of Structural Chemistry. - 2014. - Vol.55, №1. - С. 112-119. - Bibliogr. : p. 118-119 (46 ref.) Рубрики: ХИМИЧЕСКИЕ НАУКИ Кл.слова (ненормированные): POLYIODIDES -- 2-ALLYLTHIOQUINOLINE -- IODOCYCLIZATION Аннотация: Iodocyclization products of 2-allylthioquinoline are obtained in the form of polyiodides with different stoichiometric compositions. X-ray crystallography data are analyzed for two different crystal structures of 1-iodomethyl-1,2- dihydro[1,3]thiazolo[3,2-a]quinolinium polyiodides: triiodide C 12H11INS+I 3 - and complex polyiodide 2(C12H11INS+I 3 -)·I2. A comparison is made of the nonbonding interactions of dihydrothiazoloquinolinium with atoms of the triiodide anion and complex polyiodide to show the crystal structure features attributed to the participation of molecular iodine. \\\\expert2\\nbo\\Journal of Structural Chemistry\\2014, V. 55, N 1, p.112-119.pdf |
F 97 Fundamental absorption edge of NiO nanocrystals [Electronic resource] / V. I. Sokolov, A. V. Druzhinin, D. G. Kim, N. B. Gruzdev, A. Ye. Yermakov, M. A. Uimin, I. V. Byzov, N. N. Shchegoleva, V. B. Vykhodets, T. E. Kurennykh // Physica B: Condensed Matter . - 2013. - Vol. 430. - С. 1-5. - Bibliogr. : p. 5 (29 ref.) Рубрики: ХИМИЧЕСКИЕ НАУКИ Кл.слова (ненормированные): TRANSITION METAL OXIDE -- OPTICAL PROPERTIES -- CHARGE TRANSFER TRANSITIONS Аннотация: NiO nanocrystals with the average size of 5, 10 and 25 nm were synthesized by gas-condensation method. The well-defined increase of the optical density D near the fundamental absorption edge of NiO nanocrystals in the range of 3.5–4.0 eV observed after the annealing in air is caused by the oxygen content growth. It is the direct experimental evidence of the fact that p—d charge transfer transitions form the fundamental absorption edge \\\\expert2\\NBO\\Physica B\\2013, v.430, p. 1-5.pdf |
R 30 Reaction of S-allyl and propargyl derivatives of 2-thiouracils with hydrobromic acid [Electronic resource] / T. V. Frolova, D. G. Kim, V. V. Sharutin, K. Yu. Osheko, P. A. Slepukhin, V. N. Charushin // Russian Journal of General Chemistry. - 2016. - Vol. 86, № 6. - С. 1288-1291 Рубрики: ХИМИЧЕСКИЕ НАУКИ Кл.слова (ненормированные): 2-ALKENYLTHIO-4(3h)-PYRIMIDINONES -- HYDROBROMIC ACID -- 2-PROPARGYLTHIO-4(3h)-PYRIMIDINONES Аннотация: Hydrobromic acid reacts with 2-methallylthio- and 2-prenylthio-4(3De)-pyrimidinones with participation of the double bond to give the products of heterocyclization, and with 2-allylthio- and 2-propargylthio-6-methyl-4(3De)-pyrimidinones, with the retention of the double bond and the formation of hydrobromides \\\\expert2\\NBO\\Russian Journal of General Chemistry\\2016, V. 86, N 6, p. 1288-1291.pdf |