S 17 Saloutin, V. I. Transesterification of copper (II) beta-ketoesterates and acylpyruvates with borneol [Electronic resource] / V. I. Saloutin, P. N. Kondrat'ev, Z. E. Skryabina // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 1993. - Vol. 42, N 5. - P858-860 Рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: Transesterification of copper (II) acetoacetates, copper (II) trifluoroacetoacetate, and copper (II) acylpyruvates with borneol gives the copper (II) chelates of the corresponding bornyl esters in 92-95% yelds \\EXPERT2\NBO\Russian Chemical Bulletin\1993, 42 (5), 858.pdf, \\\\expert2\\NBO\\Russian Chemical Bulletin\\1993, 42 (5), 858.pdf |
N 89 Novel fluorinated chromones [Text] / V. I. Saloutin, Z. E. Skryabina, I. T. Bazyl, O. N. Chupakhin // Journal of Fluorine Chemistry. - 1993. - Vol. 65, N 1-2. - P37-41 Рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: The self-condensation of ethyl pentafluorobenzoylacetate leads to the formation of 3-pentafluorophenyl-1H-sopyrono[2,3-b]-6,7,8,9-tetrafluorochrom in 37% yeld. On hydrolysis, this gave 2-pentafluorobenzoylmethyl-5,6,7,8-tetrafluorochromone |
H 99 Interaction of fluorine-containing 1,3-dicarbonyl compounds with polyamines [Electronic resource] / V. I. Saloutin, Z. E. Skryabina, Ya. V. Burgart, S. V. Kiseleva // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 1992. - Vol. 41, N 11. - P2046-2050 Рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: In the reaction of fluorinated copper (II) 1,3-diketonates with diethylenetriamine (or triethylenetetramine) in CHC13, N,N'-bis (1,3-aminovinylketones) are formed in 21-35% yields. Fluorine-containing 1,3-diketones and 1,3-ketoesters, upon interaction with polyamines without solvent, undergo acid cleavage, forming the corresponding amides \\\\Expert2\\nbo\\Russian Chemical Bulletin\\1992, 41 (11), 2046.pdf |
A 10 A new approach to the synthesis of fluorinated chromones [Electronic resource] / V. I. Saloutin, I. T. Bazyl, Z. E. Skryabina, V. M. Krokhalev, O. N. Chupakhin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 1992. - Vol. 41, N 9. - P1714-1715 Рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: The condensation of two molecules of ethyl pentafluorobenzoylacetate gives 1-oxo-3-penta fluorophenyl-1H-pyrano[4,3-b]6,7,8,9-tetrafluorochrome \\\\Expert2\\nbo\\Russian Chemical Bulletin\\1992, 41 (9), 1714.pdf |
L 79 Liquid-phase oxidation of anthracene by hydrogen-peroxide in the presence of heterogenized vanadyl acetylacetonate [Electronic resource] / S. Y. Men'shikov, A. V. Vurasko, L. A. Petrov, L. S. Molochnikov, A. A. Novoselova, Z. E. Skryabina, V. I. Saloutin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 1992. - Vol. 41, N 4. - P619-622 Рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: The synthesis of hetrogenized vanadyl acetylacetoonate was accomplished by alkylation of a chloromethylated styrene-divinylbenzene copolymer via activation by Co (II) complexes. The effect of heterogenization of the structure of the complexes and their catelytic properties in the peroxide oxidation of anthracene was investigated by kinetic studies and ERP spectroscopy \\\\Expert2\\nbo\\Russian Chemical Bulletin\\1992, 41 (4), 619.pdf |
B 96 Burgart, Ya. V. Template reactions of fluorine-containing 1.3-diketones with ethylenediamine [Electronic resource] / Ya. V. Burgart, Z. E. Skryabina, V. I. Saloutin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 1991. - Vol. 40, N 9. - P1849-1853 Рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: Depending on the nature of the dicarbonyl fragment, the ethylenediamine and its monoprotonated salts under mild conditions gives N,N'-ethylenebis(aminovinyl ketones) and/or 1,4-diazepines \\\\Expert2\\nbo\\Russian Chemical Bulletin\\1991, 40 (9), 1849.pdf |
T 44 Thermal-decomposition of peroxide derivatives of polyfluorinated beta-ketoesters [Electronic resource] / A. I. Rakhimov, V. V. Chapurkin, A. I. Valdman, D. I. Valdman, V. I. Saloutin, K. I. Pashkevich, S. L. Kokorin, Z. E. Skryabina, // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 1990. - Vol. 39, N 7. - P1496-1499 Рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: The thermal flow microcalorimetric method was used to determine the kinetic parameters for the thermal decomposition of peroxide derivatives of polyfluorinated beta-ketoesters and the decomposition products were established \\\\Expert2\\nbo\\Russian Chemical Bulletin\\1990, 39 (7), 1496.pdf |
C 73 Conformational structure of esters of fluorinated acylpyruvic acids [Electronic resource] / P. N. Kondrat'ev, Z. E. Skryabina, V. I. Saloutin, M. N. Rudaya, T. A. Sinitsyna, K. I. Pashkevich // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 1990. - Vol. 39, N 6. - P1273-1277 Рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: Esters of fluorinated acylpyruvic acids were obtined for the first time. PMR and IR spectroscopy, dipole moment measurements, and quantum chemical calculations showed that these compounds exist as equilibrium mixtures of E and Z enolic isomers \\\\Expert2\\nbo\\Russian Chemical Bulletin\\1990, 39 (6), 1273.pdf |
R 30 Reactions of copper (II) polyfluorinated beta-diketonates and beta-ketoesterates with hydrazines [Electronic resource] / P. N. Kondrat'ev, Z. E. Skryabina, V. I. Saloutin, K. I. Pashkevich, N. A. Klyuev, G. G. Alexandrov // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 1990. - Vol. 39, N 3. - P561-565 Рубрики: ХИМИЧЕСКИЕ НАУКИ \\\\Expert2\\nbo\\Russian Chemical Bulletin\\1990, 39 (3), 561.pdf |
C 91 Crystalline hydrogen-bonded adducts of dimethyl sulphoxide and 7-hydroxypolyfluoroquinolones (chromones [Text] / V. I. Saloutin, I. T. Bazyl, Z. E. Skryabina, G. G. Alexandrov, O. N. Chupakhin // Journal of Fluorine Chemistry. - 1995. - V. 74. - P15-19 Рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: A stable crystalline hydrogen-bonded adduct of dimethyl sulphoxide (DMSO) and 7-hydroxy-5,6,8-trifluoro-2-carboxychromone has been prepared by the reaction of 2-carboxy-5,6,7,8-tetrafluorochromone with KOH/glycerol in DMSO. It has been found that pentafluorophenol and also 1-cyclohexyl-7-hydroxy-5,6,8-trifluoro-4(1H)-4-oxoquinoline-2-carboxylic acid form the corresponding crystalline hydrogen-bonded adducts with DMSO. The structure of the latter has been established from an X-ray crystallographic study |
H 99 Interaction of pentafluorobenzoylpyrunicacid and its esters with N-nucleophiles. Synthesis of Y-oxoquinoline-2-carboxylic acids [Text] / V. I. Saloutin, Z. E. Skryabina, I. T. Bazyl, P. N. Kondrat'ev, O. N. Chupakhin // Journal of Fluorine Chemistry. - 1994. - Vol. 69, № 1. - P119-126 Рубрики: ХИМИЧЕСКИЕ НАУКИ |
S 17 Saloutin, V. I. Condensation of Fluoroalkyl-containing 1,3-Dicarbonyl Compounds with Ethylendiamine [Text] / V. I. Saloutin, Z. E. Skryabina, Ya. V. Burgart // Journal of Fluorine Chemistry. - 1992. - Vol. 56, № 3. - P325-334. Рубрики: ХИМИЧЕСКИЕ НАУКИ Кл.слова (ненормированные): КОНДЕНСАЦИЯ -- СОЕДИНЕНИЯ ФТОРАЛКИЛСОДЕРЖАЩИЕ -- ФТОРАЛКИЛСОДЕРЖАЩИЕ СОЕДИНЕНИЯ -- СОЕДИНЕНИЯ 1.3-ДИКАРБОНИЛЬНЫЕ -- 1.3-ДИКАРБОНИЛЬНЫЕ СОЕДИНЕНИЯ -- этилендиамины -- ОРГАНИЧЕСКАЯ ХИМИЯ -- ХИМИЯ ОРГАНИЧЕСКАЯ |
H 99 Interaction of perfluorent-2-ene and its 2-amino-4-ivino derivative with ethylenediamine and with diethylenetriamine [Text] / V. I. Saloutin, Z. E. Skryabina, Ya. V. Burgart, O. N. Chupakhin, M. Fontaltaba, X. Solans, M. Fontbardia // Journal of Fluorine Chemistry. - 1994. - Vol. 69, N 1. - P25-29 Рубрики: ХИМИЧЕСКИЕ НАУКИ |
S 98 Synthesis of fluoroalkyl-containing 2-oxyimino-1,3-dicarbonyl compounds and their reaction with hydrazine hydrate [Text] / V. I. Saloutin, Ya. V. Burgart, Z. E. Skryabina, O. G. Kuzueva // Journal of Fluorine Chemistry. - 1997. - Vol. 84, N 2. - P107-111 Рубрики: ХИМИЧЕСКИЕ НАУКИ |
I-69 Interaction of 3-ethoxycarbonyl(carboxy)-substituted 5,6,7,8-tetrafluorochromones with N-nucleophiles synthesis of fluorocoumarins [Text] / V. I. Saloutin, Z. E. Skryabina, I. T. Bazyl, S. P. Kisil' // Journal of Fluorine Chemistry. - 1999. - Vol. 94, N 1. - P83-90 Рубрики: ХИМИЧЕСКИЕ НАУКИ |
S 98 Synthesis of Novel Fluorinated Quinolones [Text] : доклад, тезисы доклада / Z. E. Skryabina, G. A. Obanin, Ya. V. Burgart, V. I. Saloutin // International Memorial I.Postovsky Conference on Organic Chemisty, Ekaterinburg, March 17-20, 1998 : program and abstracts. - Ekaterinburg, 1998. - P52 Рубрики: ХИМИЧЕСКИЕ НАУКИ |
S 98 Synthesis of N-substituted 2-(5,6,7,8-tetrafluoro-4-oxo-1,4-dihydroquinolin-3-yl)glyoxylic acids [Electronic resource] / G. A. Obanin, A. S. Fokin, Ya. V. Burgart, O. V. Ryzhkov, Z. E. Skryabina, V. I. Saloutin, O. N. Chupakhin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 2000. - Vol. 49, № 7. - P1231-1236 Рубрики: ХИМИЧЕСКИЕ НАУКИ Кл.слова (ненормированные): ETHYL PENTAFLUOROBENZOYLPYRUVATE -- SYNTHESIS Аннотация: Methods for the synthesis of the earlier unknownN-substituted 2-(5,6,7,8-tetrafluoro-4-oxo-1,4-dihydroquinolin-3-yl)glycoxylic acids their esters from copper chelate of ethyl pentafluorobenzoylpyruvate were developed. The structure of intermediate ethyl 4-(R-amino)-2-oxo-3-pentafluorobenzoylbut-3-enoates is discussed \\\\Expert2\\nbo\\Russian Chemical Bulletin\\2000, 49 (7), 1231.pdf |
S 66 Skryabina, Z. E. Cyclization of fluoroalkyl-containing 1,3-dicarbonyl compounds with ethylenediamine hydroperchlorate to 1,4-diazepines [Electronic resource] / Z. E. Skryabina, Ya. V. Burgart, V. I. Saloutin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 1991. - Vol. 40, № 4. - P788-794 Рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: 2,3-Dihydro-1H-1,4-diazepines and 1,2,3,4-tetrahydro-1,4-diazepin-5-ones were obtained by direct condensation of fluorine-containing 1,3-diketones and 1,3-keto ethers, respectively, with ethylenediamine monohydroperchlorate. The structure of the compounds was confirmed by1H NMR, mass spectrometry and molecular weight determination \\\\Expert2\\nbo\\Russian Chemical Bulletin\\1991, 40 (4), 788.pdf |
R 30 Reaction of 2-amino-4-imino-2-perfluoropentene with ethylenediamine and diethylenetriamine [Electronic resource] / V. I. Saloutin, Z. E. Skryabina, Ya. V. Burgart, O. N. Chupakhin // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 1993. - Vol. 42, № 10. - P1697-1700 Рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: The transamination of 2-amino-4-imino-2-perfluoropentene with ethylenediamine gives the corresponding 6-fluoro-5,7-bis(trifluoromethyl)-2,3-dihydro-1H-1,4-diazepine. The transamination of 2-amino-4-imino-2-perfluoropentene by diethylenetriamine is accompanied by intramolecular nucleophilic substitution of the ?-fluorine atom to form 1,9-bis(trifluoromethyl)-3,4,6,7-tetrahydro-2H-pyrazino[1,2-a]pyrazine whose structure was established by an X-ray structural investigation. Several salts of this bicyclic compound and its complex with BF3 have been described \\\\Expert2\\nbo\\Russian Chemical Bulletin\\1993, 42 (10), 1697.pdf |
S 17 Saloutin, V. I. New fluorine-containing polyazaheterocycles [Electronic resource] / V. I. Saloutin, Z. E. Skryabina, Ya. V. Burgart // Russian Chemical Bulletin (Translation of Izvestiya Akademii Nauk, Seriya Khimicheskaya). - 1992. - Vol. 41, № 9. - P1700-1703 Рубрики: ХИМИЧЕСКИЕ НАУКИ Аннотация: Interaction of perfluoropentene-2 with ethylenediamine, diethylenetriamine, and triethylenetetramine forms previously unknown fluorine-containing azaheterocycles in yields of 25–74%. The structure of the compounds obtained has been confirmed by1H and19F NMR methods and mass spectrometry \\\\Expert2\\nbo\\Russian Chemical Bulletin\\1992, 41 (9), 1700.pdf |